New single-shot X-ray technique makes magnetic image

Aug 31, 2012 by Mike Ross
New single-shot x-ray technique makes magnetic image
An image of a nanoscale ferromagnetic structure made using a new single-shot X-ray holography technique perfected at the Soft X-ray Materials Science instrument at SLAC’s Linac Coherent Light. Image: Tianhan Wang

(—Scientists working at SLAC's Linac Coherent Light Source have captured the first single-shot X-ray microscope image of a magnetic nanostructure and shown that it can be done without damaging the material.

This result not only demonstrates the success of a powerful new X-ray technique, but it also means that in the future researchers should be able to make movies showing tiny in the act of switching polarity, the process at the heart of computer hard-disk drives and future magnetic memory technologies. Understanding the details of magnetic switching could lead to faster, denser and more energy-efficient data storage devices.

The research involved a team of 42 scientists from 16 institutions in five countries, and their results were published in the June edition of Physical Review Letters. The paper's first author is Tianhan Wang, a SLAC graduate student and member of the Stanford Institute for Materials and Energy Sciences (SIMES). Former SIMES researcher Andreas Scherz, now a scientist at the European X-Ray in Germany, was the principal investigator.

The experiments took place at the LCLS's Soft X-Ray Materials . Scientists aimed ultrashort pulses of specially prepared at a sample made of 40 alternating layers of the metals cobalt and palladium, each layer less than a nanometer thick. Before hitting the sample, the X-ray beam was circularly polarized – that is, converted to  waves that look like corkscrews, rotating around the beam either to the left or the right.

Because circularly polarized X-rays are absorbed differently by magnetic regions that are oriented "up" or "down," they have been used for many years to image the of materials in the .

The question facing the scientists was whether they could achieve a delicate balance: single X-ray pulses strong enough to create a detailed image, yet not so energetic that they would alter the sample's magnetic structure. If it worked, it should be possible in the future to make multi-shot image sequences showing magnetic changes in the same sample.

The answer was an unqualified yes.

In their experiments, the scientists varied the length and intensity of the X-ray pulses. They found that the longer pulses heated the sample and changed its magnetic structure. But good images with no damage to the sample resulted from shorter pulses ­– 80 femtoseconds, or quadrillionths of a second, long ­– with energy fluence of 5-25 millijoules per square centimeter.

"We were delighted to find such a big window of acceptable energy density," Wang said. "Our results confirm that we should be able to make sequential, ultrafast X-ray images of a single sample."

Wang anticipates that future research will include a detailed examination of how visible laser light can switch magnetic domains, which could lay the foundation for optically switched magnetic hard-disk drives. Today's disk drives use electrically generated magnetic fields to write and erase data.

"To increase data density, the bits on a magnetic hard disk have to be made smaller," Wang said. "But magnetic bits are already so small that they're nearly unstable. More stable magnetic materials would be much more difficult to erase and rewrite data, which is undesirable."

While laser light can be used to switch some of these stable materials, "we don't know enough details to be able to control the process," Wang said. "This new X-ray technique should enable us to make the measurements we need to gain such insight."

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