X-ray laser experiment explores how specially shocked material gets stronger

April 23, 2014 by Glenn Roberts Jr.
Despina Milathianaki, a staff scientist at SLAC's LCLS, holds a series of titanium alloy samples prepared for an experiment. The experiment was designed to study the laser-shocked state of the materials. Credit: Fabricio Sousa/SLAC

(Phys.org) —Rolls-Royce researchers came to SLAC earlier this month as part of a team testing titanium and titanium alloys such as those used in engine parts, landing gear and other aircraft components.

While the Rolls-Royce brand is also associated with luxury cars, this separate company, Rolls-Royce PLC, is a major global manufacturer of aircraft engines that power over 30 types of commercial aircraft. It is the first industrial user of SLAC's Linac Coherent Light Source X-ray laser since LCLS opened to visiting scientists in October 2009.

"Understanding materials is what drives innovation in the materials," said Michael G. Glavicic, a materials specialist for Rolls-Royce Corp. in Indianapolis, who led the experiment with David Dye of Imperial College London.

Ultimately, Glavicic said, "We want to understand what happens to a material when it's in an engine. The more we know about how an alloy behaves, the more we can be creative and figure out ways to take advantage of those properties."

The company's researchers often partner with laboratories and universities to explore hybrid materials that could find their way into products. In this case they are seeking a deeper understanding of how titanium alloys behave when pushed to extremes not found in any flight test. The results could lead to ways to make the alloys even tougher.

Lightweight, super-strong and able to withstand high heat and stress, titanium is increasingly airborne; the major application of titanium alloys is in aircraft components.

Some of the members of a Rolls-Royce-led team at SLAC's LCLS X-ray laser explore shocked titanium and titanium alloys. From left: Tom Swinburne, graduate student at Imperial College London; Despina Miathianakis, LCLS staff scientist; Michael G. Glavicic, associate fellow materials at Rolls-Royce Corp.; and Garth Williams, LCLS staff scientist. Credit: Fabricio Sousa/SLAC

The LCLS experiment was designed to study the creation and growth of deformation in thin-foil samples of titanium and its alloys. Researchers hit the samples with powerful optical laser pulses at LCLS, and then used the X-ray laser to study how the material responded to this shock. The ultrashort, ultrabright X-ray laser pulses can uniquely capture images of samples at the nanoscale, and in increments measured in tens of femtoseconds (quadrillionths of a second).

One type of stress-caused deformation that researchers hoped to see forming is known as "twinning," named for mirror-image patterns that appear in the metal's microscopic structure. These twin regions are separated by thin boundaries that appear as lines. Like well-sewn seams across layers of fabric, the twin boundaries can actually strengthen the material.

An equipment table at the Coherent X-ray Imaging (CXI) experimental station at SLAC's LCLS. The equipment was put to use in an experiment studying the shocked state of titanium and titanium alloys. Credit: Fabricio Sousa/SLAC

"This is something that nobody has done before in that we're hoping to see 'twins' form – see the rate at which they form, to understand what role chemistry plays in causing things to twin," Glavicic said. "It could potentially confirm or build on current theories."

Researchers hope to use deformation mechanisms that are now considered a hindrance to improve how materials withstand stress. While commercial applications from such an experiment may be decades away, Glavicic said the goal is to gain fundamental insights about material properties that can be shared with the scientific community.

The sample chamber at the Coherent X-ray Imaging experimental station at SLAC's LCLS. Credit: Fabricio Sousa/SLAC

"LCLS is uniquely suited to this type of experiment," said Despina Milathianaki, an LCLS staff scientist involved in the research, "because the deformation processes often evolve in trillionths of a second," or picoseconds. The tiny focus and coherence of the LCLS X-ray pulses, she said, also allow scientists to capture images within a single "crystallite" or grain in the metal, which is an individual building block in a metal's structure.

"We hope that this is the first of many collaborations with industry partners seeking to understand fundamental materials science by exploiting the unique capabilities of LCLS," Milathianaki added.

Explore further: Copper shock: An atomic-scale stress test

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