PNNL’s Shear Assisted Processing and Extrusion™, or ShAPE, technology. Credit: Andrea Starr /Pacific Northwest National Laboratory

Two forms of magnesium material that were processed into tubing using a novel manufacturing technology called Shear Assisted Process and Extrusion—or ShAPE—were found to have quite similar and improved microstructures, even though they began vastly different.

This finding confirms that PNNL's ShAPE technology can extrude components directly from low-cost castings and deliver improved microstructures compared to conventional extrusion processes. The results could mean lower-cost and potentially higher-performing product for the automotive, aerospace, and other industries.

This research, conducted by and engineers from Pacific Northwest National Laboratory, was published in Materials Science and Engineering: A.

It's All About the Processing

Automotive manufacturers are investigating lighter-weight materials to replace heavier aluminum and steel automotive components. One alternative——has the potential for 80 percent weight savings compared to steel, and 30 percent savings as opposed to the already-lightweight aluminum.

However, magnesium alloys have only accounted for 0.5 percent of a typical passenger vehicle's weight during the past two decades.

That's because magnesium typically needs to be reinforced with to bolster its energy absorption properties. Unfortunately, rare earth elements are costly—more than 10 times the cost of without rare earth elements.

To investigate how processing non-rare earth element-containing—and inexpensive—magnesium feedstocks impact extruded product performance, the PNNL team turned two feedstock materials into tubes using the ShAPE technology and then performed analyses on the tubes.

Billets and Bars

The two feedstocks the team processed and analyzed were ZK60 magnesium in the as-cast form and in the "cold-worked" T5 condition.

As-cast billets consist of a mix of metals that were melted and then solidified in a casting—primarily magnesium but also containing zinc, zirconium, and very small amounts of other metals. The casting contains grains of magnesium and other phases, with a range of sizes.

T5-conditioned bars are cold worked from the casting, being processed through an extruder to form a bar shape, and then heat treated. The resulting grain size, texture, and second-phase particles significantly differ from those in the as-cast form.

The team used ShAPE to process the as-cast billets and T5-conditioned bars into tubing under similar process conditions. ShAPE uses a rotating die that is "rammed" against a container holding the magnesium material, causing frictional heating at the die-material interface. As the , the material softens—but does not melt—and flows toward the extrusion opening through spiral grooves machined into the die face to form tubes.

The tubes produced for this study had an outer diameter of 50.8 mm (2 in.) and a wall thickness of 1.9 mm (0.07 in.). They were produced using greater than 20 times less the ram force compared to conventional extrusion methods.

Analyses of both materials following ShAPE processing showed that the microstructures were virtually identical, suggesting that the end product is independent of the starting form of the magnesium alloy. These microstructures were indistinguishable from previously reported ZK60 tubes extruded using ShAPE, where twice the ductility was achieved compared to conventionally extruded material. This exciting result indicates that ShAPE can be used to extrude products directly from low-cost castings, in a single step, while still achieving properties that exceed those of conventionally extruded tubing.

"The results indicate that magnesium alloy extrusions may be fabricated directly from castings, with microstructures that are higher performing than can be achieved with conventional extrusion methods—and without the high cost of rare earth elements," said PNNL materials scientist Scott Whalen, who led the study. "Going directly from castings can reduce, or even eliminate, the need for energy-intensive heat treatment processes required prior to performing conventional extrusion."

ShAPE is part of PNNL's growing suite of capabilities in Solid Phase Processing—or SPP, a disruptive approach to metals manufacturing that can be better, cheaper, and greener than melt-based methods typically associated with metals manufacturing.

More information: S. Whalen et al. Magnesium alloy ZK60 tubing made by Shear Assisted Processing and Extrusion (ShAPE), Materials Science and Engineering: A (2019). DOI: 10.1016/j.msea.2019.04.013