Magnetic actuation enables nanoscale thermal analysis

Jan 12, 2012
This is the atomic force microscope with an integrated heater actuated using Lorentz forces. Credit: William King

Polymer nano-films and nano-composites are used in a wide variety of applications from food packaging to sports equipment to automotive and aerospace applications. Thermal analysis is routinely used to analyze materials for these applications, but the growing trend to use nanostructured materials has made bulk techniques insufficient.

In recent years an atomic force microscope-based technique called nanoscale thermal analysis (nanoTA) has been employed to reveal the temperature-dependent properties of materials at the sub-100 nm scale. Typically, nanothermal analysis works best for soft polymers. Researchers at the University of Illinois at Urbana-Champaign and Anasys Instruments, Inc. have now shown that they can perform nanoscale thermal analysis on stiff materials like epoxies and filled composites.

"This new technique lets us measure temperature and frequency-dependent properties of materials rapidly over a wide bandwidth," noted William King, the College of Engineering Bliss Professor in the Department of Mechanical Science and Engineering at Illinois, who led the research. The technique works by flowing a current around the U-shaped arms of a self-heating (AFM) cantilever and interacting that current with a magnetic field. The magnetic field allows the tip-sample force to be modulated right near the tip of the AFM.

"We are able to achieve nanometer-scale force control that is independent from the heating temperature," according to Byeonghee Lee, first author of the paper.

"Conventional nanothermal analysis has struggled with highly filled, highly crosslinked materials and sub-100 nm . This new technique has allowed us to reliably measure and map and melting transions on classes of materials that were previously very challenging," said Craig Prater, at Anasys Instruments and co-author on the paper.

Explore further: Engineers' nanoantennas improve infrared sensing

More information: "Magnetic Actuation of a Heated Atomic Force Microscope Cantilever using Lorentz Force," Nanotechnology doi:10.1088/0957-4484/23/5/055709

Related Stories

Researchers measure nanometer scale temperature

Dec 19, 2011

Illinois researchers have developed a new kind of electro-thermal nanoprobe that can independently control voltage and temperature at a nanometer-scale point contact. It can also measure the temperature-dependent ...

A New Way Forward for Nanocomposite Nanostructures

Feb 24, 2010

(PhysOrg.com) -- Scientists at the Naval Research Laboratory and the University of Illinois-Urbana Champaign recently reported a new technique for directly writing composites of nanoparticles and polymers.

Femtogram-level chemical measurements now possible

Mar 27, 2008

Finding a simple and convenient technique that combines nanoscale structural measurements and chemical identification has been an elusive goal. With current analytical instruments, spatial resolution is too low, signal-to-noise ...

NIST imaging system maps nanomechanical properties

Dec 12, 2007

The National Institute of Standards and Technology has developed an imaging system that quickly maps the mechanical properties of materials—how stiff or stretchy they are, for example—at scales on the ...

Researchers ink nanostructures with tiny 'soldering iron'

Nov 07, 2011

Researchers with the Lawrence Berkeley National Laboratory (Berkeley Lab) have shed light on the role of temperature in controlling a fabrication technique for drawing chemical patterns as small as 20 nanometers. ...

Recommended for you

Engineers' nanoantennas improve infrared sensing

16 hours ago

(Phys.org) —A team of University of Pennsylvania engineers has used a pattern of nanoantennas to develop a new way of turning infrared light into mechanical action, opening the door to more sensitive infrared ...

Stacking 2-D materials produces surprising results

May 16, 2013

(Phys.org) —Graphene has dazzled scientists, ever since its discovery more than a decade ago, with its unequalled electronic properties, its strength and its light weight. But one long-sought goal has proved ...

User comments : 0

More news stories

Engineers' nanoantennas improve infrared sensing

(Phys.org) —A team of University of Pennsylvania engineers has used a pattern of nanoantennas to develop a new way of turning infrared light into mechanical action, opening the door to more sensitive infrared ...

Advance in nanotech gene sequencing technique

(Phys.org) —The allure of personalized medicine has made new, more efficient ways of sequencing genes a top research priority. One promising technique involves reading DNA bases using changes in electrical ...

Lab sets a new record for creating heralded photons

(Phys.org) —Entanglement, by general consensus of physicists, is the weirdest part of quantum science. To say that two particles, A and B, are entangled means that they are actually two parts of an inseparable ...

Protein study suggests drug side effects are inevitable

A new study of both computer-created and natural proteins suggests that the number of unique pockets – sites where small molecule pharmaceutical compounds can bind to proteins – is surprisingly small, meaning drug side ...

Do salamanders hold the solution to regeneration?

Salamanders' immune systems are key to their remarkable ability to regrow limbs, and could also underpin their ability to regenerate spinal cords, brain tissue and even parts of their hearts, scientists have ...